Particle size analysis providers in Chelmsford, MA? ?We partner with companies in all phases of product development and sales, including R&D, manufacturing, QC, advertising and failure analysis. Our laboratory offers a highly-trained and experienced staff utilizing a powerful set of analytical tools (SEM with EDS and backscatter detectors, Bruker X-Flash elemental mapping, X-Ray imaging, Micro-FTIR spectroscopy, Micro-XRF, light microscopy, cross sectioning/precision polishing and microhardness testing).
The desired chip packages were sectioned from the larger board, and placed in an epoxy mounting cup. The epoxy was mixed and allowed to harden. The resulting epoxy puck was cross sectioned and polished. The epoxy mounting and cross sectioning process gave precise, perfectly preserved cross sectional surfaces through the desired components and their solder bonds. Read extra details on eds elemental analysis.
Dust samples were analyzed using polarized light microscopy (PLM) to provide percentages of the particle types present in the samples. MVL was able to determine that there was significant loading of glass fibers in the dust samples with the likely source being contractor’s work in the attic which involved disturbing the fiberglass insulation. The image on the right shows a few distinct glass fibers with a binder material adhered to them, consistent with fiberglass insulation.
What is your standard turnaround time (TAT) and can it be expedited? Our standard TAT is 5 to 10 business days. We can provide faster TATs on request with the following surcharges: – Same day to 24 hour rush is 100% surcharge – 2 day rush is 75% surcharge – 3 day rush is 50% surcharge – 4 day rush is 25% surcharge Rush requests must have prior approval otherwise we cannot guarantee turnaround times.
Using light microscopes to examine the optical and structural properties of samples is one of the oldest and most useful analytical techniques. MicroVision Labs has several high magnification microscopes, including a powerful Zeiss Axiotech microscope capable of 1800x optical magnification, with additional digital magnification, allowing for visualization of sub-micron structures. PLM allows for the identification of a wide range of particles through the examination of the internal birefringence, or variation in optical indices, within a sample. Explore a few extra info on https://microvisionlabs.com/.
As indicated in the FTIR spectral comparison below, the suspect material showed a near perfect match for acetylsalicylic acid. Additionally, there was a small amount of dibasic phosphate present. It was determined that the material was likely acetylsalicylic acid with a phosphate binder – an aspirin. Therefore, from this analysis the suspect material in the bottle was likely a household aspirin tablet, broken apart and separated by the water. In order to confirm the identification, a few aspirin tablets from several common manufacturers were obtained, roughly ground, and soaked to allow for comparison. The optical morphology of the crystals, size range of the particles, association with the phosphate and FTIR spectrum all were consistent with the original suspect material. A report detailing the methods and findings in full narrative form was rendered to the client.